Thesis Abstract

Abstract
Metal-organic frameworks (MOFs) have attracted significant attention in recent years due to their unique properties and potential applications in gas storage. This thesis focuses on the synthesis and characterization of novel MOFs for gas storage applications. The research aims to explore the design and synthesis of MOFs with enhanced gas storage capacities and selectivities. The study involves the development of new synthetic strategies, characterization techniques, and evaluation of gas adsorption properties. Chapter One provides an introduction to the research area, including the background of the study, problem statement, objectives, limitations, scope, significance, structure of the thesis, and definition of key terms. The literature review in Chapter Two covers ten key aspects related to MOFs, gas storage, synthesis methods, characterization techniques, and applications in gas separation. The research methodology in Chapter Three outlines the experimental procedures, materials, and equipment used in the synthesis and characterization of MOFs. Chapter Four presents a detailed discussion of the findings, including the synthesis routes employed, structural characterization data, gas adsorption isotherms, and evaluation of gas storage capacities. The results highlight the importance of structural design and synthetic parameters in tailoring the gas adsorption properties of MOFs. The discussion also explores the implications of the findings for potential gas storage applications. In the final chapter, Chapter Five, the conclusion and summary of the thesis are provided. The key findings, implications, limitations, and future research directions are discussed. Overall, this thesis contributes to the field of MOFs for gas storage applications by presenting novel synthesis strategies, detailed characterization data, and insights into enhancing gas adsorption properties. The research outcomes provide valuable knowledge for the development of advanced MOFs with improved gas storage capacities and selectivities. Keywords Metal-organic frameworks, MOFs, gas storage, synthesis, characterization, gas adsorption, gas separation, porous materials, adsorption properties.

Thesis Overview

The project titled "Synthesis and characterization of novel metal-organic frameworks for gas storage applications" aims to explore the development of advanced materials known as metal-organic frameworks (MOFs) for the purpose of gas storage. This research overview provides a comprehensive explanation of the project, outlining the significance, objectives, methodology, and potential impact of the study. Metal-organic frameworks (MOFs) are a class of porous materials composed of metal ions or clusters connected by organic linkers. These materials exhibit high surface areas, tunable pore sizes, and unique chemical properties, making them promising candidates for various applications, including gas storage. The specific focus of this project is on the synthesis and characterization of novel MOFs tailored for efficient gas storage, with a particular emphasis on enhancing the storage capacity, selectivity, and stability of these materials. The primary objective of this research is to design and synthesize novel MOFs with superior gas storage capabilities compared to existing materials. This involves exploring different metal ions, organic linkers, and synthesis methods to create MOFs with optimized properties for storing gases such as hydrogen, methane, or carbon dioxide. The characterization of these MOFs will involve a range of analytical techniques, including X-ray diffraction, nitrogen sorption analysis, and thermal gravimetric analysis, to elucidate their structural features, porosity, and stability. The research methodology encompasses a series of experimental steps, starting from the selection of metal ions and organic linkers based on their compatibility and reactivity. The synthesis of MOFs will be carried out using solvothermal or hydrothermal methods, with careful control over reaction conditions to achieve the desired crystal structure and morphology. Characterization techniques will be employed to analyze the physical and chemical properties of the synthesized MOFs, providing insights into their gas sorption capacities and storage performance. The findings of this study are expected to contribute to the advancement of MOF materials for gas storage applications, offering insights into the design and synthesis of tailored frameworks with enhanced gas adsorption properties. The discussion of results will focus on the relationship between MOF composition, structure, and gas storage performance, highlighting key factors that influence the adsorption capacity and selectivity of these materials. Additionally, the implications of the research findings for potential industrial applications and future research directions will be explored. In conclusion, the project on the synthesis and characterization of novel metal-organic frameworks for gas storage applications represents a significant contribution to the field of materials science and energy storage technology. By developing advanced MOF materials with improved gas storage capabilities, this research has the potential to address challenges in gas storage and separation, paving the way for the design of efficient and sustainable energy storage systems.